2D NMR study of solution conformations and complete H-1 and C-13 chemical shifts assignments of vitamin D metabolites and analogs

MD Mizhiritskii; LE Konstantinovskii; R Vishkautsan

doi:10.1016/0040-4020(95)00954-X

Back

2D NMR study of solution conformations and complete H-1 and C-13 chemical shifts assignments of vitamin D metabolites and analogs

Journal article

Peer reviewed

2D NMR study of solution conformations and complete H-1 and C-13 chemical shifts assignments of vitamin D metabolites and analogs

MD Mizhiritskii, LE Konstantinovskii and R Vishkautsan

Tetrahedron, Vol.52(4), pp.1239-1252

Jan/1996

DOI: https://doi.org/10.1016/0040-4020(95)00954-X

Files and links (2)

url

https://doi.org/10.1016/0040-4020(95)00954-XView

Published (Version of record) Restricted

url

https://ezproxy.weizmann.ac.il/login?url=http://dx.doi.org/10.1016/0040-4020(95)00954-XView

Published (Version of record) Restricted

Abstract

In addition to conventional 1D H-1 and C-13 NMR, including DEFT and NOE methods, 2D-shift-correlated NMR techniques (H-1-H-1 COSY and H-1-C-13 HMQC) were used, providing an approach to the complete signal assignments for vitamin D analogs and model compounds. On the basis of NMR data,solution conformations of vitamin D and analogs were studied.

Details

Title: 2D NMR study of solution conformations and complete H-1 and C-13 chemical shifts assignments of vitamin D metabolites and analogs
Creators: MD Mizhiritskii (null)
LE Konstantinovskii (null)
R Vishkautsan (null)
Resource Type: Journal article
Publication Details: Tetrahedron, Vol.52(4), pp.1239-1252; Jan/1996
Number of pages: 14
Language: English
DOI: https://doi.org/10.1016/0040-4020(95)00954-X
Record Identifier: 993266991303596

Metrics

16 Record Views